Thursday, December 11, 2014

EXPERIMENT 1.1 : BALL MILLING



OBJECTIVES:

1. To determine the particle size distribution of the coarse salt. 
2. To observe the effect of speed and time in grinding the coarse salt.

INTRODUCTION :

Ball milling process is introduces as a process to reduce the particle size or in other grinding process. This process is used to grind materials to small fine particles and is widely use especially in the mineral dressing processes, paints and ceramics industries. The grinders that are used are from different materials including the ceramic balls, flint pebbles and stainless steel balls. 

This process works by the effective speed by which the balls rotating along with the cylindrical pot and an internal cascading effect of the balls reduce the materials size to small powders. 

 MATERIALS AND APPARATUS:
  • 300.4179 g of coarse salt
  • Steel ball
  • Ball mill
  • Sieve nest
  • Weighing balance

PROCEDURE:

1) 313.980 of coarse salts were weighed
2) Different sizes of steel balls were inserted to the mill.
3) The weighed salts were inserted into the mill.
4) The milling process was initiated with the speed of 10 within 20 minutes.
5) The product obtained is then weighed again after the milling process ended.
6) The powder obtained was sieved using the sieving method with sieve nest. 
7) Results data was collected and a histogram was plotted.        




RESULTS:









DISCUSSION: 
         
Firstly, during weighing the course salts, we may observed the reading wrongly. We also may insert different size of steel ball into the cylindrical shell which may affect the reduction size as the larger size ball will crush the particulates better compare to the smaller ball size. Therefore, not all the coarse salts are reduced with same efficiency. We also may not adjust the speed relatively with the time causing the coarse salts not completely grind to even distribution of fines.

Other factors affecting the particles size reduction process are the size of grinding media. A smaller size would result in even smaller size of final product. Besides that,  the hardness of the grinding media, the stickiness of grinding media, the density of grinding media also effect the process. Other equipment that can be used to reduce the size particle is Hammer milling, fluid energy milling, and Colloid mill. 

All of this equipment used the mechanism of impact to reduce the size of particulate. In choosing the right equipment for size reduction process, one of the factor influences is the nature of the raw materials.  Most of the raw material must be dried before undergo the reduction process. Other than that, establishing the particle size required are also important to avoid undesired particle size formed due to incorrect choosing of right equipment. The product from the milling process is subjected for particle size analysis


QUESTIONS:

1) What are the factors that can influence the size reduction process of a ball mill?
  • The number and size of the steel balls used in the milling process.
  • The speed of the ball milling process.

2)What are the other equipment that can be used in size reduction of solid materials?
  • Hammer milling, fluid energy milling, and colloid mill. 

3)What are the factors that need to be considered in choosing the suitable size reducing 

    equipment?
  • The nature of the raw materials.

CONCLUSION : 

As the aim of this experiment is to study the effect of the various parameters on the performance of a ball mill. The factors studied are particle size,, time of grinding, and speed of the ball mill (rpm).  From the results, we can conclude that the amount of fine particles increase with the increase in time of grinding, speed (rpm) of the ball milling process. 


REFERENCES:

A ball mill for all grinding and milling needs. http://www.retsch.com/products/sumo/mixerball-millphp/ [24 November 2014]

Cao W. Synthesis of Nanomaterials by High Energy Ball Milling. http://www.understandingnano.com/nanomaterial-synthesis-ball-milling.html [25 November 2014]



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